By S. Greenfield, M. Clift, R. Belcher, H. Freiser
Analytical Chemistry of the Condensed Phosphates describes the idea that and mode of operation of assorted analytical equipment for research of the condensed phosphates.
This ebook consists of ten chapters, and starts off with a presentation of the final homes of the condensed phosphates. massive chapters are dedicated to quite a few analytical ideas used for condensed phosphate research, corresponding to gravimetry, titrimetry, and electrometric, chromatographic, actual, and automatic tools. A bankruptcy discusses the methods for the selection of esters of the condensed phosphates. The concluding chapters survey the popular approach to quantitative research of those compounds, in addition to the education of natural samples.
This ebook will turn out invaluable to analytical, inorganic, and natural chemists and researchers.
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Extra resources for Analytical Chemistry of the Condensed Phosphates
Eng. Chem. 44, 615 (1952). 61. H U H T I , A. L. and GARTAGANIS, P. , Can. J. Chem. 34, 785 (1956). 62. VAN WAZER, J. R. , / . Am. Chem. Soc. 8 1 , 6360 (1959). 63. THILO, E. , / . Prakt. Chem. 4 , 324 (1957). 64. 65. 66. 67. , RIEMAN, W. , Analyt. Chem. 26, 505 (1954). WESTMAN, A. E. , SCOTT, A. E. and PEDLEY, J. , Chem. in Canada, 4, 35 (1952). VAN WAZER, J. R. and HOLST, K. , / . Am. Chem. Soc. 72, 639 (1950). ANDRESS, K. , GEHRING, W. , Z. anorg. allgem. Chem. 260, 331 (1949). 68. , SCHULZ, G.
Chem. 27, 401 (1955). , ICHIDA, H . , Kyoto Yakka Daigaku Gakuho 5, 36 (1957). 14. , Mem. Fac. , Ser. C, 2, 161 (1957). 15. BRAZIER, J. R , Ph. D . , England (1967). 16. VAN WAZER, J. R. and CAMPANELLA, D . , J. Am. Chem. Soc. 72, 655 (1950). 17. , HAGIWARA, Z. , Technol. Rep. Tohoku Univ. 26,1 (1956). 18. EBEL, J. P. , 239, 173 (1954). 19. EBEL, J. , COLAS, J. and BUSCH, R , Bull. Soc. chim. France, 1087 (1955). 5 ; and N a 3 P 3 0 9 and "hexameta" from pH 6, with sodium hydroxide solution. From further aliquots at the same pH the curves were completed by titrating with hydrochloric acid solution.
Allow to settle for 12 hours, filter and store in the dark. Orthophosphate colour standard. 0 g of ferric alum in 85 ml of concentrated hydrochloric acid, dilute to 1000 ml and add a further 100 ml of concentrated hydrochloric acid and 900 ml of water. 0200 g of Na 2 HP0 4 per 100 ml by means of the procedure described under (b) below. 00 g of sample in 20 ml of water contained in a 500 ml centrifuge tube. Add 20 ml of 2 N hydrochloric acid followed by 5 ml of benzidine reagent. If no precipitate forms, long-chain phosphates are absent.
Analytical Chemistry of the Condensed Phosphates by S. Greenfield, M. Clift, R. Belcher, H. Freiser